NWI-MOL122
Chemical Analysis 2
Cursus informatieRooster
CursusNWI-MOL122
Studiepunten (ECTS)3
CategoriePB (Propedeuse)
VoertaalEngels
Aangeboden doorRadboud Universiteit; Faculteit der Natuurwetenschappen, Wiskunde en Informatica; Moleculaire Wetenschappen;
Docenten
Coördinator
dr. M. Tessari
Overige cursussen docent
Docent
dr. M. Tessari
Overige cursussen docent
Contactpersoon van de cursus
dr. M. Tessari
Overige cursussen docent
Examinator
dr. M. Tessari
Overige cursussen docent
Collegejaar2021
Periode
KW2  (08-11-2021 t/m 30-01-2022)
Aanvangsblok
KW2
Onderwijsvorm
voltijd
Opmerking-
Inschrijven via OSIRISJa
Inschrijven voor bijvakkersJa
VoorinschrijvingNee
WachtlijstNee
Plaatsingsprocedure-
Cursusdoelen
Upon completion of this course the students are able to:
  • explain the operating principles, strengths and limitations of the following analytical techniques:
            Atomic Absorption and Emission Spectroscopy
            Infrared Spectroscopy
            Mass Spectrometry
            Nuclear Magnetic Resonance Spectroscopy
  • describe the main components and relative properties (source, detector, ...) of routinely employed spectrometers for each technique.
  • discuss applications of analytical chemical techniques and choose the appropriate method for a given analytical problem.
Inhoud
  • Atomic UV-Vis spectroscopy: temperature and the Boltzmann distribution, linewidths (Heisenberg uncertainty principle, Doppler effect, pressure broadening), hollow cathode lamp, ICP, background and interference corrections. 
  • Infrared Spectroscopy: selection rules, Fourier transformation (qualitative), dispersive spectrometer vs. FT spectrometer, radiation sources, detectors, window materials, sample preparation, measurement techniques.   
  • Ion sources, mass analyzers, detectors, hyphenated mass spectrometry, Total Ion Current, Extracted Ion Current, Single Ion Monitoring, applications: element analysis, radiocarbon dating.   
  • Shielding/de-shielding high/low field shift, FT NMR (spin, magnetic field, precession, radio waves, resonance, single pulse, hard pulse, 90° pulse, detection, FID, Fourier transformation), weak vs. strong coupling, dihedral angles, heteronuclear NMR, MRI.
Instructional Modes
Niveau

Voorkennis
NWI-MOL121 Chemical Analysis 1 NWI-MOL120 Structure of Atoms and Molecules
Toetsinformatie
The examination consists of three intermediate digital tests, roughly at 1/3, 2/3 and at the end of the second quarter. These intermediate tests replace the final exam at the end of the course.  The average mark must be equal to or above 6 to pass. Students must enroll for each intermediate test.

Students that do not take all three intermediate tests or have an average mark below 6 can take the resit, also in the form of a digital exam.

Grading will be in accordance with RU standards, on a scale of 1 to 10. The final grade is rounded to the nearest half, with the exception of grades between 5.0 and 6.0 which are rounded to the nearest integer. Grades of 6 and higher are considered a 'pass' and grades lower than 6 are considered a 'fail'.
Bijzonderheden

Verplicht materiaal
Boek
ISBN:978-1-4641-3538-5
Titel:Quantitative Chemical Analysis, 9th ed., 2016, New York
Auteur:D.C. Harris
Uitgever:W.H. Freeman and Company
Boek
ISBN:978-0-1987-69866
Titel:Atkins’ Physical Chemistry 11th edition
Auteur:Peter Atkins, Julio de Paula
Uitgever:Oxford University Press

Werkvormen
Hoorcollege

Werkcollege

Toetsen
Digital Exam (resit)
Weging1
ToetsvormDigitale toets met CIRRUS
GelegenhedenBlok KW2

Digital Partial Exam 1
Weging1
ToetsvormDigitale toets met CIRRUS
GelegenhedenBlok KW2

Digital Partial Exam 2
Weging1
ToetsvormDigitale toets met CIRRUS
GelegenhedenBlok KW2

Digital Partial Exam 3
Weging1
ToetsvormDigitale toets met CIRRUS
GelegenhedenBlok KW2